Applied Chemical Engineering
In present work, a heterogeneous Fenton process using prepared Fe2O3@ CeO2; 1:2 ratio /AC nanocatalyst was used to treat wastewater discharged from Iraqi petroleum refinery plant. The heterogeneous Fenton process was evaluated for its efficiency in removing COD via application a response surface methodology (RSM) and adopting a batch mode. Three essential operating factors were considered namely …
Herein, two new azo reagents, 2-[(1-banzimidazol)azo]-2-hydroxy-5-banzal (BIApB) and 6-[(1-banzethiazol) azo thymol] (BTAT), were synthesized and identified using FTIR, UV-Vis, mass spectrometry, and ¹H-NMR. Also, this research presents a comparative analysis of novel azo-chelating reagents for the cloud point extraction (CPE) of gold complexes. The study evaluates how the structural differences …
This study presents a chemical engineering-based analysis of transport phenomena in porous media, focusing on the coupled mechanisms of fluid flow and solute migration within an unlined canal system. The work is framed within environmental chemical engineering, where seepage is interpreted not only as a hydraulic loss but also as a transport-driven mechanism governing solute migration, adsorption…
Cadmium sulfide (CdS) thin films were successfully synthesized using thiourea as the sulfur precursor through the spray pyrolysis technique for photovoltaic (PV) applications. The structural, optical, and photoluminescence properties of the films were investigated to assess their suitability as an electron transport layer (ETL) in perovskite solar cells. X-ray diffraction (XRD) analysis confirmed…
This work studied the production of biodiesel from waste cooking oil using an ultrasonic reactor and the testing of biodiesel fuel performance in a diesel engine on a light truck. The process for biodiesel production consisted of several steps, including waste cooking oil filtration, esterification, ultrasonic-assisted transesterification, biodiesel separation using the decantation process, washi…
This study conducts a strategic stakeholder analysis of Morocco’s Advanced Metering Infrastructure (AMI) within the country’s broader energy-transition reforms. It employs a qualitative triangulation design, combining semi-structured interviews, deep documentary analysis, and relational mapping. Results highlight a centralised governance pattern in which public institutions, international donors,…
Background: The increasing demand for plant-based dairy alternatives has highlighted almond milk as a popular option due to its favorable sensory properties and suitability for individuals with lactose intolerance or milk protein sensitivity. However, its inherently low levels of calcium and vitamin D3 limit its nutritional equivalence to cow’s milk, particularly in populations with higher minera…
Three new Schiff base compounds (S1-S3) from 1-([1,1'-biphenyl]-4-yl)ethan-1-amine and substituted-benzaldehydes are synthesized and biologically evaluated in this work. After microwave-assisted synthesis, the compounds were purified and structurally characterized by FTIR, 1H-NMR, and 13C-NMR. Agar diffusion was used to test their antibacterial activities against pathogens such Staphylococcus aur…
This determined the electrical characteristics of the six-naphthalene bridge tetracyanoquinodimethane dye that were suggested. The characteristics were determined by plotting energy and temperature against one another. The SIESTA-trunk-426 program was used for the relaxation of the dyes under study by employing the Generalized Gradient Approximation/Double Zeta Density Functional Theory (GGA/DZ-D…
This paper examines some of the properties and potential applications of montmorillonite, which is a type of clay in the smectite group, and its importance in achieving some of the Sustainable Development Goals. This paper points to some of the unique attributes that the mineral has, most of which lie in its capacity to retain water and provide essential nutrients, thus improving soil quality. So…
Through a Vilsmeier–Haack condensation 2-chloro-3-formyl-1.8-nathyridine (I) was synthesized. When treated with aqueous hydrochloric acid converted to compound (II) was successfully obtained in high yield and then converted to Novel 1-(8-methyl) furo[2,3-b] -(1,8-naphthyridine-2-yl) ethenone (III) through Claisen –Schmidt condensation. The condensation between compound III (ketone) and benzaldehy…
Iron plays a pivotal role in hematopoiesis, particularly in hemoglobin synthesis and oxygen transport. Alterations in iron availability, whether nutritional or pharmacological, directly influence erythroid indices and red blood cell morphology. This study employed validated UV–Vis spectrophotometric methods combined with hematological analysis to evaluate the effects of iron-containing substances…
Salbutamol sulfate was analyzed using a straightforward, expeditious, and precise spectrophotometric approach. This method enabled the rapid and precise quantification of salbutamol sulfate within complex samples.in this method Salbutamol sulfate is coupled with a diazotized p-methoxy aniline reagent in an alkaline medium to form stable and water- soluble yellow azo dye . The resulting compound e…
Prodrug based on polymers are pictured macromolecules and these prodrugs performance unique angle to raise the solubility and pharmacokinetics and pharmacological properties. According to their benefits as anticancer drugs, the highlights focused on the synthesis of prodrug polymers and their applications in medicine field, So these polymers having degradable amide bonds linked to paracetamol and…
Extraction is critical step in extracting bioactive phytochemicals from plant sources and separating them. In this study, a Box-Benken (BBD) design was used, with 15 experiments conducted to optimize the ultrasonic extraction process. Three independent variables (ethanol concentration, temperature, and time) were examined to assess their effect on total extract yield (TYE) as the main response. T…
The sewage treatment systems in the cities demand small and efficient technologies that can eliminate both traditional and emerging pollutants. However, the practical use of the high-technology adsorbents in real-life situations of municipal wastewater is still limited. Engineering usage of high-performance adsorbents, such as the granular activated carbon (GAC), activated biochar, and Fe₃O₄-func…
Heavy metal contamination in agricultural soil poses a significant threat to food safety and public health. This study investigated the concentrations of Lead (Pb) and Iron (Fe) in various plant species and their associated soils at the Al-Kifil site compared to a control site (Al-Ibrahimiya). Soil and plant samples (Onion, Swiss Chard, Broad Beans, Spinach, Garden Cress, and Barley) were analyze…
Pomegranate peel is a natural considerable agro-industrial waste with high polyphenolics and essential minerals which can be used as functional ingredients. This work also suggests the green analytical approach comprising natural deep eutectic solvents (NaDES) coupled with UAE for effective recovery of polyphenols from pomegranate peel along with ICP-MS for multi-element mineral profiling and UV-…
In this study a new organic Schiff base-azo ligand was prepared using two steps the condensation and diazotization reaction, this ligand used for reacting with the copper (II) ion to form a copper complex and determination small amounts of it, the prepared ligand and complex were characterized by UV-Vis, FT-IR, 1HNMR spectra, also measured Molar electrical conductivity for complex. Ion copper (II…
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